Single-Course Engelsk 5 ECTS

Organic and Inorganic Synthesis

Overall Course Objectives

To practice laboratory techniques with particular emphasis on syntheses of organic and inorganic compounds, including separation and purification. To use spectroscopic methods for compound identification. To use kemibrug for assessment and evaluation of the risk factors for the chemicals used. To practice a safe behaviour in the laboratory.

See course description in Danish

Learning Objectives

  • Assemble synthetic apparatus using standard laboratory glassware
  • Carry out simple organic and inorganic syntheses
  • Separate organic compounds using extraction and distillation
  • Perform purification of the synthetic products by crystallisation and/or distillation
  • Write experimental records in a laboratory notebook in a way that will allow the experiment to be reproduced
  • Analyse the synthetic products by qualitative, spectroscopic (IR, optical rotation) and physical methods (melting point, boiling point)
  • Use gas chromatography, gravimetric analysis and titration for determination of purity
  • Explain and understand the theory behind the reactions performed
  • Be familiar with practical work in the laboratory
  • Use Kemibrug for evaluation of risk factors for the compounds used
  • Work safely in the chemical laboratory

Course Content

Synthesis of organic and inorganic compounds. Simple synthetic techniques are employed for separation and purification of the synthesised compound, e.g. distillation, filtration, recrystallisation, drying and extraction. Analysis and characterisation of the synthesised compounds by spectroscopic (IR) and chromatographic (GC) methods. Notebook writing. Safety in the laboratory, including familiarity with practical work.

Possible start times

  • 36 – 49 (Wed 8-17)
  • 36 – 49 (Mon 13-17)
  • 36 – 49 (Tues 8-12)
  • 6 – 20 (Wed 8-17)
  • 6 – 20 (Mon 13-17)
  • 6 – 20 (Tues 8-12)

Recommended prerequisites

26471, 26471 Organic chemistry or equivalent.

Teaching Method

Laboratory course

Limited number of seats

Maximum: 24.

Please be aware that this course has a limited number of seats available. If there are too many applicants, a pool will be created for the remainder of the qualified applicants, and they will be selected at random. You will be informed 8 days before the start of the course, whether you have been allocated a spot.

See course in the course database.

Registration

Language

Engelsk

Duration

13 weeks

Institute

Chemistry

Place

DTU Lyngby Campus

Course code 26474
Course type Graduate Engineer
Price

9.250,00 DKK

Please note that this course has participants limitation. Read more

Registration